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中国科学院福建物质结构研究所氘代还原工作被百年书刊Organic Syntheses收录（图）
中国科学院福建物质结构研究所 氘代 还原工作 百年书刊 Organic Syntheses 收录
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2021/4/1
中科院福建物构所鲍红丽课题组在国家重点研发计划（2017YFA0700103）、国家自然科学基金（21672213,21871258,21922112）和中科院战略性先导科技专项（XDB20000000）等项目支持下，近期提出了一个巧妙的策略，即利用廉价的氘水作为氘源，通过极性反转策略将羰基还原氘代，以良好的收率和高的氘代率制备α-氘代醇（图二）。该体系仅需1.5当量的氘水，成本仅为现有技术的百分...
Oxorhenium(V)-mediated syntheses and structures of oxypyridinium-ammonium zwitterions
Oxorhenium(V) oxypyridinium-ammonium zwitterions
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2010/4/8
Treatment of N,N-bis(2-hydroxybenzyl)-2-(2-aminoethyl) dimethylamine (H2had) with trans-[ReO2(py)4]I in acetone affords the iodide salts of the oxypyridinium-ammonium zwitterions N1-(2-hydroxybenzyl)-...
Use of Silicon Substituents in the Syntheses of Natural and Non-natural Molecules
trimethylsilyl ulky group lipophilic group
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2007/12/20
摘要 Trimethylsilyl groups have been used in our research as a director as well as a bulky and lipophilic group in our quest for natural and non-natural molecules.
Solid-state syntheses of M-Cu-S (M = Mo and W) clusters, crystal structure and nonlinear optical properties of {MS4[Cu(p-MeOC6H4)3P]2}.0.5C6H12
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2007/7/28
专著信息
书名
Solid-state syntheses of M-Cu-S (M = Mo and W) clusters, crystal structure and nonlinear optical properties of {MS4[Cu(p-MeOC6H4)3P]2}.0.5C6H12
语种
英文
撰写或编译
作者
Zheng,H. G.,Zhou,J. L.,Tan,W. L.,...
Great Framework Variation of Polymers in the Manganese(Ⅱ) Maleate/a,a-Diimine System: Syntheses,Structures, and Magneto-Structural Correlation,
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2007/7/28
专著信息
书名
Great Framework Variation of Polymers in the Manganese(Ⅱ) Maleate/a,a'-Diimine System: Syntheses,Structures, and Magneto-Structural Correlation,
语种
英文
撰写或编译
作者
C. Ma,C. Chen,Q. Liu,F. Chen,D. ...
Syntheses of Disordered and Al-rich Hydrotalcite-Like Compounds
Syntheses of Disordered Al-rich Hydrotalcite-Like Compounds
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2012/1/12
Hydrotalcite-like compounds, [Mg1−xAlx(OH)2]x+ [xX− · n H2O], where X− = ½ CO32- or OH−, were prepared by hydrothermal syntheses at PH2O = 100 MPa and T = 100°–350°C. St...
Syntheses of Glauconite at Surface Temperatures
Glauconite Diagenesis Pore solutions Synthesis
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2012/2/9
Glauconite has been synthesized at low temperature by precipitation of Fe-hydroxides from Si-, Fe-, Al-, and K-containing solutions under reducing conditions. The compositions favorable for the synthe...
The Syntheses of Hydrotalcite-Like Compounds and Their Structures and Physico-Chemical Properties I: The Systems Mg2+-Al3+-NO3−, Mg2+-Al3+-Cl−, Mg2+-Al3+-ClO4−, Ni2+-Al3+-Cl− and Zn2+-Al3+-Cl−
Syntheses Hydrotalcite-Like Compounds Physico-Chemical Properties
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2012/2/15
The basic salts of this system were prepared and their structures and physico-chemical properties were studies by electron microscopy, chemical analysis, X-ray powder diffraction, thermal analysis, i....
Hydrothermal Syntheses of Amino Acid-Montmorillonites and Ammonium-Micas
Hydrothermal Syntheses Amino Acid-Montmorillonites Ammonium-Micas
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2012/2/13
An attempt has been made to synthesize nitrogenous clay minerals hydrothermally from silica-alumina gels in the presence of amino acids, namely glycine and lysine. The products have been characterized...